3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇合成路线 （共 69 条）
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647-42-73,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇
反应条件
1: 83 percent / TBAF / tetrahydrofuran 2: LiHBEt3 / tetrahydrofuran / 2 h / 20 °C View Scheme
参考文献
Molecules, , vol. 9, # 5 p. 266 - 277
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647-42-73,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇+
反应条件
2-(F-hexyl)-1-iodoethane; water T=140°C; 4.5 h;
参考文献
Journal of Organic Chemistry, , vol. 58, # 7 p. 1804 - 1811
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647-42-73,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇+
反应条件
water T=140°C; 4.5 h;
参考文献
Journal of Organic Chemistry, , vol. 58, # 7 p. 1804 - 1811
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647-42-73,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇+
反应条件
pyrrolidin-2-one; potassium carbonate 1.) 140 deg C, 6.00 h, 2.) EtOH, CHCl3, 68 deg C, 5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 60, # 7 p. 2059 - 2071
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647-42-73,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇+
反应条件
water T=130°C; 7 h; Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 61, # 19 p. 6504 - 6516
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647-42-73,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇+
反应条件
water T=141°C; 3 h; Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 61, # 19 p. 6504 - 6516
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647-42-73,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇+
反应条件
water; silver nitrate; copper(II) sulfate T=180°C; Gas phase; Conversion of starting material;
参考文献
US6664430 B1, ;
Page column 8-9 ;
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647-42-73,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇+
反应条件
T=140°C; 7.25 h; Yields of byproduct given;
参考文献
Brace
Journal of Organic Chemistry, 1995 , vol. 60, # 7 p. 2059 - 2071
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647-42-73,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇+
反应条件
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-iodooctane; water; potassium carbonate 1) 141 deg C, 3 h, 2) acetone, CHCl3, 66 deg C, 4 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 61, # 19 p. 6504 - 6516
→
647-42-73,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇+
反应条件
solution aqueuse de soude 10 N 0.25 h; Heating;
参考文献
Tetrahedron, , vol. 37, p. 487 - 492
