3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇 合成路线 (共 69 条)
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647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇
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Yield given. Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 29, p. 119
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647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇 +
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water T=140°C; 1 h; var. temp., time, substrate (DMF, 1,2-ethanyl-bis-formamide) investigated; Product distributionRate constant;
参考文献
Journal of Fluorine Chemistry, , vol. 31, p. 151 - 174
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647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇 +
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water Product distribution;
参考文献
Journal of Fluorine Chemistry, , vol. 29, p. 119
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647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇 +
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T=140°C; 1 h; other times; also with ε-caprolactam; Rate constantMechanism;
参考文献
Journal of Organic Chemistry, , vol. 60, # 7 p. 2059 - 2071
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647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇 +
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T=140°C; 1 h; var. temp., time, substrate (DMF) investigated; Product distributionRate constant;
参考文献
Journal of Fluorine Chemistry, , vol. 31, p. 151 - 174
647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇
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air; chlorine T=22.85°C; P=750 Torr; UV-irradiation; Product distribution;
参考文献
Ellis, David A.; Martin, Jonathan W.; De Silva, Amila O.; Mabury, Scott A.; Hurley, Michael D.; Sulbaek Andersen, Mads P.; Wallington, Timothy J.
Environmental Science and Technology, 2004 , vol. 38, # 12 p. 3316 - 3321
647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇 +
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sodium hydroxide; tetra-(n-butyl)ammonium iodide in water T=45°C; 48 h;
参考文献
Malkov, Andrei V.; Figlus, Marek; Stoncius, Sigitas; Kocovsky, Pavel
Journal of Organic Chemistry, 2007 , vol. 72, # 4 p. 1315 - 1325
647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇
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1: bis(trichloromethyl) carbonate With pyridine in pentane T=-15°C; 1 h; 2: 3,3,4,4,5,5, 6,6,7,7,8,8,8-tridecafluorooctanol in pentane T=-15 - 20°C; 6 h;
参考文献
Vincenti, Marco; Ghiglione, Nicoletta; Valsania, Maria Carmen; Davit, Patrizia; Richardson, Susan D.
Helvetica Chimica Acta, 2004 , vol. 87, # 2 p. 370 - 375
647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇
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phosphoric acid; phosphorus pentoxide; potassium iodide T=120°C; 4 h;
参考文献
Peroche, Sandrine; Parrot-Lopez, Helene
Tetrahedron Letters, 2003 , vol. 44, # 2 p. 241 - 245
647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇 +
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in diethyl ether T=0 - 20°C; 12 h;
参考文献
Massi, Lionel; Guittard, Frederic; Levy, Richard; Duccini, Yves; Geribaldi, Serge
European Journal of Medicinal Chemistry, 2003 , vol. 38, # 5 p. 519 - 523