7-(羧基甲氧基)-4-甲基香豆素合成路线 (共 11 条)
反应条件
sodium hydroxide in ethanol; water 2 h; Heating;
参考文献
Chimichi, Stefano; Boccalini, Marco; Cosimelli, Barbara
Tetrahedron, 2002 , vol. 58, # 24 p. 4851 - 4858
反应条件
1: 57.5 g / K2CO3; tetrabutylammonium bromide / acetone / 18 h / 30 °C 2: LiOH; water / tetrahydrofuran View Scheme
参考文献
Arzneimittel-Forschung/Drug Research, , vol. 53, # 12 p. 857 - 863
反应条件
sodium hydroxide 2 h; Heating;
参考文献
Eltamany, S. H.; El-Deen, I. M.; El-Fattah, M. E. Abd
Pakistan Journal of Scientific and Industrial Research, 1995 , vol. 38, # 3-4 p. 115 - 118
反应条件
sodium hydroxide 1 h; Heating;
参考文献
Karlsson, Karl-Erik; Wiesler, Donald; Alasandro, Mark; Novotny, Milos
Analytical Chemistry, 1985 , vol. 57, # 1 p. 229 - 234
反应条件
methanol; potassium chloride; sodium chloride; calcium chloride; sodium hydroxide; magnesium chloride; 2-[4-(2-hydroxyethyl)-1-piperazinyl] ethanesulfonic acid in water pH=7.2; Photolysis; Quantum yieldKinetics; Wavelength;
参考文献
Tetrahedron, , vol. 68, # 38 p. 8024 - 8032
参考文献
Rybalkin; Popova; Dubonosov; Shepelenko; Revinskii; Bren'; Minkin
Russian Journal of Organic Chemistry, 2001 , vol. 37, # 9 p. 1318 - 1322
反应条件
1: sulfuric acid / water / 17 h / 20 °C 2: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C 3: hydrogenchloride; water; acetic acid / 0.5 h / Reflux View Scheme
参考文献
Tetrahedron, , vol. 68, # 38 p. 8024 - 8032
反应条件
1: With triethylamine in N,N-dimethyl-formamide; toluene Curtius rearrangement; 3 h; Heating; 2: With potassium hydroxide; glycerol in ethanol; N,N-dimethyl-formamide; toluene 2 h; Heating; Further stages.;
参考文献
Spurg, Anke; Waldvogel, Siegfried R.
European Journal of Organic Chemistry, 2008 , # 2 p. 337 - 342
反应条件
1: 75 percent / H2SO4 / benzene / 14 h / Heating 2: 63 percent / hydrazine hydrate / ethanol / 4 h / Heating View Scheme
参考文献
Eltamany, S. H.; El-Deen, I. M.; El-Fattah, M. E. Abd
Pakistan Journal of Scientific and Industrial Research, 1995 , vol. 38, # 3-4 p. 115 - 118
反应条件
sulfuric acid in benzene
14 h; Heating;
参考文献
Eltamany; El-Deen; El-Fattah, M. F. Abd
Journal of the Indian Chemical Society, 1996 , vol. 73, # 7 p. 367 - 369
Title/Abstract Full Text View citing articles Show Details
Eltamany, S. H.; El-Deen, I. M.; El-Fattah, M. E. Abd
Pakistan Journal of Scientific and Industrial Research, 1995 , vol. 38, # 3-4 p. 115 - 118