3,4,4-三甲氧基-2,5-环己二烯-1-酮合成路线 （共 10 条）
反应条件
(-)-10-CSA; water Inert atmosphere;
参考文献
Goodell, John R.; McMullen, Jonathan P.; Zaborenko, Nikolay; Maloney, Jason R.; Ho, Chuan-Xing; Jensen, Klavs F.; Porco Jr., John A.; Beeler, Aaron B.
Journal of Organic Chemistry, 2009 , vol. 74, # 16 p. 6169 - 6180
反应条件
potassium carbonate; bis-[(trifluoroacetoxy)iodo]benzene in acetonitrile
0.166667 h; Ambient temperature;
参考文献
Tamura, Yasumitsu; Yakura, Takayuki; Haruta, Jun-ichi; Kita, Yasuyuki
Journal of Organic Chemistry, 1987 , vol. 52, # 17 p. 3927 - 3930
反应条件
oxalic acid in tetrahydrofuran; water
0.2 h; Ambient temperature; Yield given;
参考文献
Evans; Tanis; Hart
Journal of the American Chemical Society, 1981 , vol. 103, # 19 p. 5813 - 5821
反应条件
acetic acid in tetrahydrofuran; water
参考文献
Dolson, Mark G.; Swenton, John S.
Journal of Organic Chemistry, 1981 , vol. 46, # 1 p. 177 - 179
反应条件
[bis(acetoxy)iodo]benzene; silica gel; triethylamine
T=20°C; 5 h;
参考文献
Bodipati, Naganjaneyulu; Peddinti, Rama Krishna
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 23 p. 4549 - 4553
反应条件
[bis(acetoxy)iodo]benzene; silica gel; triethylamine
T=20°C; 6 h;
参考文献
Bodipati, Naganjaneyulu; Peddinti, Rama Krishna
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 23 p. 4549 - 4553
反应条件
acetic acid
1) MeOH, electrolyzed, 15 deg C, 2 h, 2) acetone, 45 min, room temperature; Yield given. Multistep reaction. Further byproducts given;
参考文献
Henton, Daniel R.; Anderson, Keith; Manning, Michael J.; Swenton, John S.
Journal of Organic Chemistry, 1980 , vol. 45, # 17 p. 3422 - 3433
反应条件
[bis(acetoxy)iodo]benzene
参考文献
Yin, Zhiwei; Zhang, Jinzhu; Wu, Jing; Green, Riana; Li, Sihan; Zheng, Shengping
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 18 p. 2854 - 2858
反应条件
[bis(acetoxy)iodo]benzene
参考文献
Hu, Yinjun; Kamitanaka, Tohru; Mishima, Yusuke; Dohi, Toshifumi; Kita, Yasuyuki
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5530 - 5543
反应条件
(i) nBuLi, (ii) /BRN= 2051746/, (iii) BF3-Et2O; Multistep reaction;
参考文献
Evans,D.A. et al.
Journal of the American Chemical Society, 1977 , vol. 99, # 21 p. 7083 - 7085
