n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.75 h;
参考文献
Vedejs, Edwin; Naidu; Klapars, Artis; Warner, Don L.; Li, Ven-Shun; Na, Younghwa; Kohn, Harold
Journal of the American Chemical Society, 2003 , vol. 125, # 51 p. 15796 - 15806
1.1: iPr2NH; n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C
1.2: 93 percent / tetrahydrofuran; hexane / -78 - 20 °C
2.1: 57 percent / n-BuLi / tetrahydrofuran; hexane / 0.75 h / -78 °C
View Scheme
参考文献
Vedejs, Edwin; Naidu; Klapars, Artis; Warner, Don L.; Li, Ven-Shun; Na, Younghwa; Kohn, Harold
Journal of the American Chemical Society, 2003 , vol. 125, # 51 p. 15796 - 15806
