三丁基(2-乙氧基乙烯基)锡合成路线 （共 10 条）
参考文献
US2004/122018 A1, ;
Page 156 ;
反应条件
tert.-butyl lithium in diethyl ether; pentane T=-78°C; 1.11667 h;
参考文献
WO2007/24593 A1, ;
Page/Page column 50 ;
WO 2007/024593 A1
反应条件
boron trifluoride diethyl etherate in dichloromethane T=-78°C; 1 h;
参考文献
Cabezas, Jorge A.; Oehischlager, Allan C.
Tetrahedron Letters, 1995 , vol. 36, # 29 p. 5127 - 5130
反应条件
bis-triphenylphosphine-palladium(II) chloride in chloroform T=80°C; P=3800 Torr;
参考文献
Sakamoto; Yasuhara; Kondo; Yamanaka
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 5 p. 1137 - 1139
反应条件
bis-triphenylphosphine-palladium(II) chloride; tetraethylammonium chloride; oxalic acid 1.) MeCN, reflux, 4 h, 2.) MeCN, reflux, 3 h; Multistep reaction;
参考文献
Sakamoto, Takao; Yasuhara, Akito; Kondo, Yoshinori; Yamanaka, Hiroshi
Heterocycles, 1993 , vol. 36, # 11 p. 2597 - 2600
反应条件
boron trifluoride diethyl etherate in dichloromethane T=-78°C; var. Lewis acids; Product distribution;
参考文献
Tetrahedron Letters, , vol. 36, # 29 p. 5127 - 5130
反应条件
bis-triphenylphosphine-palladium(II) chloride; tetraethylammonium chloride in N,N-dimethyl-formamide T=80°C; 2 h; var. solvents and temp., other aromatic bromides; Product distribution;
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Yasuhara, Akito; Yamanaka, Hiroshi
Heterocycles, 1990 , vol. 31, # 2 p. 219 - 221
反应条件
boron trifluoride diethyl etherate in dichloromethane T=-78°C; 1 h;
参考文献
Cabezas, Jorge A.; Oehischlager, Allan C.
Tetrahedron Letters, 1995 , vol. 36, # 29 p. 5127 - 5130
反应条件
n-butyllithium in tetrahydrofuran
T=-78°C;
参考文献
Wollenberg,R.H. et al.
Journal of the American Chemical Society, 1977 , vol. 99, # 22 p. 7365 - 7367
反应条件
1: With bis-triphenylphosphine-palladium(II) chloride in acetonitrile
4 h; Heating / reflux;
2: With potassium fluoride in water; acetonitrile
T=20°C; 0.5 h;
参考文献
BANYU PHARMACEUTICAL CO., LTD.
Patent: EP1790650 A1, 2007 ;
Location in patent: Page/Page column 59 ;
