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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
64740-46-1
合成路线
（共 21 条）
109-99-9
四氢呋喃
+
64740-46-1
→
反应条件
122-97-4
3-苯丙醇
+
114302-28-2
+
103-65-1
正丙基苯
+
538-68-1
戊基苯
+
1081-77-2
正壬基苯
+
1196-58-3
3-苯基戊烷
反应条件
MechanismProduct distribution;
参考文献
Maercker, Adalbert; Passlack, Michael
Chemische Berichte, 1982 , vol. 115, # 2 p. 540 - 577
507-19-7
溴代叔丁烷
+
64740-46-1
→
反应条件
300-57-2
烯丙基苯
+
873-66-5
甲基苯乙烯
+
63213-06-9
+
40132-64-7
反应条件
in diethyl ether T=20°C; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tanaka, Jiro; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the Chemical Society, Chemical Communications, 1986 , # 3 p. 242 - 244
507-19-7
溴代叔丁烷
+
64740-46-1
→
反应条件
300-57-2
烯丙基苯
+
873-66-5
甲基苯乙烯
+
63213-06-9
+
58463-02-8
+
40132-64-7
+
74120-63-1
反应条件
in diethyl ether T=20°C; addition of TMEDA or HMPA, preferred pathway tested; Product distribution;
参考文献
Tanaka, Jiro; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the Chemical Society, Chemical Communications, 1986 , # 3 p. 242 - 244
15424-05-2
+
64740-46-1
→
反应条件
873-66-5
甲基苯乙烯
+
58463-02-8
+
74120-63-1
+
107847-57-4
反应条件
in diethyl ether T=20°C; in the absence or presence of HMPA; Product distribution;
参考文献
Tanaka, Jiro; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the Chemical Society, Chemical Communications, 1986 , # 3 p. 242 - 244
507-19-7
溴代叔丁烷
+
64740-46-1
→
反应条件
300-57-2
烯丙基苯
+
873-66-5
甲基苯乙烯
+
63213-06-9
+
40132-64-7
反应条件
in diethyl ether T=20°C; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tanaka, Jiro; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the Chemical Society, Chemical Communications, 1986 , # 3 p. 242 - 244
507-19-7
溴代叔丁烷
+
64740-46-1
→
反应条件
300-57-2
烯丙基苯
+
63213-06-9
+
58463-02-8
+
40132-64-7
反应条件
in diethyl ether T=20°C; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tanaka, Jiro; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the Chemical Society, Chemical Communications, 1986 , # 3 p. 242 - 244
507-19-7
溴代叔丁烷
+
64740-46-1
→
反应条件
300-57-2
烯丙基苯
+
63213-06-9
+
40132-64-7
+
4403-14-9
反应条件
in diethyl ether T=20°C; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tanaka, Jiro; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the Chemical Society, Chemical Communications, 1986 , # 3 p. 242 - 244
507-19-7
溴代叔丁烷
+
64740-46-1
→
反应条件
300-57-2
烯丙基苯
+
63213-06-9
+
40132-64-7
+
74120-63-1
反应条件
in diethyl ether T=20°C; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tanaka, Jiro; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the Chemical Society, Chemical Communications, 1986 , # 3 p. 242 - 244
507-19-7
溴代叔丁烷
+
64740-46-1
→
反应条件
300-57-2
烯丙基苯
+
873-66-5
甲基苯乙烯
+
63213-06-9
+
58463-02-8
+
40132-64-7
+
74120-63-1
反应条件
in diethyl ether T=20°C; addition of TMEDA or HMPA, preferred pathway tested; Product distribution;
参考文献
Tanaka, Jiro; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the Chemical Society, Chemical Communications, 1986 , # 3 p. 242 - 244
64740-46-1
→
反应条件
103-65-1
正丙基苯
+
553-54-8
苯甲酸锂
+
117657-84-8
反应条件
PhCOOD; benzoic acid in tetrahydrofuran T=-78°C; 0.5 h;
参考文献
Beak, Peter; Pfeifer, Lance A.
Journal of Physical Organic Chemistry, 1997 , vol. 10, # 7 p. 537 - 541
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