1: benzenesulphinic acid sodium salt With polystyrene-supported-SeCl in N,N-dimethyl-formamide
T=20°C; 6 h; solid-phase reaction;
2: cyclopentene With boron trifluoride diethyl etherate in dichloromethane
T=20°C; 40 h;
3: With dihydrogen peroxide in tetrahydrofuran
T=20°C; 2 h;
1: 96 percent / N-iodosuccinimide / CH2Cl2 / 20 °C
2: 92 percent / neutral alumina / CH2Cl2 / 24 h / 20 °C
View Scheme
参考文献
Wolff, Russell R.; Basava, Vikram; Giuliano, Robert M.; Boyko, Walter J.; Schauble, J. Herman
Canadian Journal of Chemistry, 2006 , vol. 84, # 4 p. 667 - 675
1: 96 percent / N-iodosuccinimide / CH2Cl2 / 20 °C
2: 92 percent / neutral alumina / CH2Cl2 / 24 h / 20 °C
View Scheme
参考文献
Wolff, Russell R.; Basava, Vikram; Giuliano, Robert M.; Boyko, Walter J.; Schauble, J. Herman
Canadian Journal of Chemistry, 2006 , vol. 84, # 4 p. 667 - 675
