2,5-二溴甲基对苯二甲腈合成路线 （共 5 条）
参考文献
de Diesbach; Zurbriggen
Helvetica Chimica Acta, 1925 , vol. 8, p. 551
反应条件
1: dimethylformamide / Heating
2: NBS / CCl4 / Heating
View Scheme
参考文献
Xiao; Yu; Chua; Huang
Chemistry - A European Journal, 2000 , vol. 6, # 8 p. 1318 - 1321
反应条件
1: bromine / dichloromethane / 18 h / 12 °C
2: N,N-dimethyl-formamide / 48 h / Reflux
3: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / 5 h / Irradiation; Reflux
View Scheme
参考文献
Zhang, Li-Na; Wu, Fang-Ying; Liu, Ai-Hong
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2011 , vol. 79, # 1 p. 97 - 103
反应条件
in chloroform
48 h; Heating / refluxIrradiation;
参考文献
Sony Corporation
Patent: US6337167 B1, 2002 ;
Location in patent: Example 11 ;
参考文献
de Diesbach; Zurbriggen
Helvetica Chimica Acta, 1925 , vol. 8, p. 551
