8-碘-4,5,7-三甲氧基-2-萘羧酸甲酯合成路线 （共 7 条）
反应条件
mercury(II) diacetate; iodine in acetic acid
T=50°C;
参考文献
Cameron, Donald W.; Feutrill, Geoffrey I.; Pannan, Linda J. H.
Australian Journal of Chemistry, 1980 , vol. 33, # 11 p. 2531 - 2541
反应条件
in trifluoroacetic acid
Ambient temperature;
参考文献
Cameron, Donald W.; Feutrill, Geoffrey I.; Pannan, Linda J. H.; Raston, Colin L.; Skelton, Brian W.; White, Allan H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 610 - 627
参考文献
Cameron, Donald W.; Feutrill, Geoffrey I.; Pannan, Linda J. H.
Australian Journal of Chemistry, 1980 , vol. 33, # 11 p. 2531 - 2541
反应条件
1: 44 percent / 230 °C
2: 1.) 48percent aq. HBr, 2.) dimethyl sulfate, K2CO3 / 1.) reflux, 3 h, 2.) acetone, reflux, 18 h
View Scheme
参考文献
Cameron, Donald W.; Feutrill, Geoffrey I.; Pannan, Linda J. H.
Australian Journal of Chemistry, 1980 , vol. 33, # 11 p. 2531 - 2541
反应条件
1: 4 percent / 230 °C
2: 14 percent / 66percent nitric acid, I2 / acetic acid / 14 - 16 °C
View Scheme
参考文献
Cameron, Donald W.; Feutrill, Geoffrey I.; Pannan, Linda J. H.
Australian Journal of Chemistry, 1980 , vol. 33, # 11 p. 2531 - 2541
反应条件
1: 4 percent / 230 °C
2: 90 percent / KOH / aq. ethanol / 4 h / Heating
View Scheme
参考文献
Cameron, Donald W.; Feutrill, Geoffrey I.; Pannan, Linda J. H.
Australian Journal of Chemistry, 1980 , vol. 33, # 11 p. 2531 - 2541
参考文献
Cameron, Donald W.; Feutrill, Geoffrey I.; Pannan, Linda J. H.; Raston, Colin L.; Skelton, Brian W.; White, Allan H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 610 - 627
