反应条件
1.1: 95 percent / DMAP
2.1: L-Selectride(R) / tetrahydrofuran / 3 h / -78 - 0 °C
2.2: tetrahydrofuran / 2 h / 25 °C
3.1: 74 percent / Pd(OAc)2; dppf / tetrahydrofuran / 6 h / 40 °C
4.1: 1,4-cyclohexadiene; H2 / Pd/C
5.1: NaCNBH3
6.1: 95 percent / TFA
View Scheme
参考文献
Tasber, Edward S.; Garbaccio, Robert M.
Tetrahedron Letters, 2003 , vol. 44, # 51 p. 9185 - 9188
