反应条件
1: 1,1-diphenylthiourea; phenyl isothiocyanate With sodium hydride in tetrahydrofuran; paraffin oil
T=45°C; Inert atmosphere;
2: With hydrogen bromide; dihydrogen peroxide in tetrahydrofuran; paraffin oil
Inert atmosphere;
3: methanesulfonyl chloride Further stages;
参考文献
Feeny, Rachel M.; Le, Diane N.; Parks, Joseph W.; Epstein, Mark G.; Pagano, Joseph V.; Abbene, Albert C.; Graham, Elaina B.; Farrell, Joanna R.; McGuire, Jason R.; Zoellner, Robert W.; Valente, Edward J.; Barklis, Eric; Wood, Warren J. L.
Synlett, 2012 , # 2 p. 301 - 305
