4-甲基苯硫代亚磺酸 S-(4-甲基苯基)酯合成路线 （共 36 条）
反应条件
18-crown-6 ether; bis-(phenyl)-sulfoxide in pyridine T=17°C; 10 h; also diaryldisulfides; var. solvent, reagents and reaction cond.; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 54, # 9 p. 2712 - 2723
反应条件
benzenesulfenyl chloride 1.) CDCl3, -10 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 37, # 50 p. 9101 - 9104
反应条件
18-crown-6 ether 1.) pyridine, 0 deg C, 30 min; 2.) H2O-MeOH, overnight, room temp.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Oae, Shigeru; Takata, Toshikazu; Kim, Yong Hae
Tetrahedron, 1981 , vol. 37, p. 37 - 44
反应条件
in benzene T=20 - 40°C;
参考文献
Poudrel, Jean-Marc; Cole, Edward R.
Phosphorus, Sulfur and Silicon and Related Elements, 2001 , vol. 175, p. 79 - 86
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in water; acetonitrile
0.333333 h;
参考文献
Vincent, Stephane P.; Burkart, Michael D.; Tsai, Chung-Ying; Zhang, Zhiyuan; Wong, Chi-Huey
Journal of Organic Chemistry, 1999 , vol. 64, # 14 p. 5264 - 5279
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane
T=0°C; Aza-Diels-Alder reaction; 1 h; Inert atmosphere; diastereoselective reaction;
参考文献
Andreassen, Trygve; Lorentzen, Marianne; Hansen, Lars-Kristian; Gautun, Odd R.
Tetrahedron, 2009 , vol. 65, # 14 p. 2806 - 2817
反应条件
in xylene
T=150°C; 0.25 h;
参考文献
Arnone, Alberto; Bravo, Pierfrancesco; Frigerio, Massimo; Viani, Fiorenza; Soloshonok, Vadim A.
Tetrahedron, 1998 , vol. 54, # 39 p. 11825 - 11840
反应条件
dihydrogen peroxide; trifluoroacetic acid; methyltrioxorhenium (VII) in water; acetonitrile
T=25°C; Oxidation; pH=1.0; KineticsProduct distribution;
参考文献
Wang, Ying; Espenson, James H.
Journal of Organic Chemistry, 2000 , vol. 65, # 1 p. 104 - 107
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane
T=-78°C; Aza-Diels-Alder reaction; 20 h; Inert atmosphere; optical yield given as percent eediastereoselective reaction;
参考文献
Andreassen, Trygve; Lorentzen, Marianne; Hansen, Lars-Kristian; Gautun, Odd R.
Tetrahedron, 2009 , vol. 65, # 14 p. 2806 - 2817
反应条件
3-cyano-1-methylquinolinium perchlorate in acetonitrile-D3
PhotolysisSchlenk technique;
参考文献
Cavattoni, Tullio; Del Giacco, Tiziana; Lanzalunga, Osvaldo; Mazzonna, Marco; Mencarelli, Paolo
Journal of Organic Chemistry, 2013 , vol. 78, # 10 p. 4886 - 4894
