1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C
1.2: 2 h / 0 - 20 °C
2.1: diisobutylaluminium hydride / dichloromethane / 2 h / 0 °C
View Scheme
参考文献
Bizet, Vincent; Pannecoucke, Xavier; Renaud, Jean-Luc; Cahard, Dominique
Journal of Fluorine Chemistry, 2013 , vol. 152, p. 56 - 61