2-(3-甲基苯基)乙烷硫胺合成路线 (共 3 条)
反应条件
hydrogenchloride; dithiophosphoric acid O,O-diethyl ester in 1,4-dioxane
T=20°C; 18 h;
参考文献
Takeda Pharmaceutical Company Limited
Patent: EP2530078 A1, 2012 ;
Location in patent: Page/Page column 191 ;
反应条件
triethylamine in pyridine; benzene
参考文献
Burroughs Wellcome Co.
Patent: US3987158 A1, 1976 ;
反应条件
Lawesson's reagent in tetrahydrofuran
1.5 h; Heating / reflux;
参考文献
BAYER HEALTHCARE AG
Patent: WO2005/97784 A1, 2005 ;
Location in patent: Page/Page column 67 ;