反应条件
1: diisobutylaluminium hydride / diethyl ether / 0 °C
2: pyridine / dichloromethane / 0 - 20 °C
3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C
4: tris-(dibenzylideneacetone)dipalladium(0); triphenylphosphine / tetrahydrofuran / 24 h / 20 °C / |Schlenk technique; |Inert atmosphere
View Scheme
参考文献
Olszewska, Beata; Kryczka, Boguslaw; Zawisza, Anna
Tetrahedron, 2013 , vol. 69, # 46 p. 9551 - 9556
