1: m-chloroperbenzoic acid / CH2Cl2 / 3 h / 28 °C 2: 95 percent / [tris(1-pyrazolyl)borate]RuPPh3(CH3CN)2PF6 / toluene / 3 h / 100 °C View Scheme
参考文献
Madhushaw, Reniguntala J.; Lin, Ming-Yuan; Abu Sohel, Shariar Md.; Liu, Rai-Shung
Journal of the American Chemical Society, 2004 , vol. 126, # 22 p. 6895 - 6899
tetrabutyl ammonium fluoride in tetrahydrofuran
T=26°C; 8 h;
参考文献
Madhushaw, Reniguntala J.; Lin, Ming-Yuan; Abu Sohel, Shariar Md.; Liu, Rai-Shung
Journal of the American Chemical Society, 2004 , vol. 126, # 22 p. 6895 - 6899
1.1: n-BuLI / tetrahydrofuran / 0.5 h / 0 °C
1.2: tetrahydrofuran / 4 h / 20 °C
2.1: Bu4NF / tetrahydrofuran / 8 h / 26 °C
View Scheme
参考文献
Madhushaw, Reniguntala J.; Lin, Ming-Yuan; Abu Sohel, Shariar Md.; Liu, Rai-Shung
Journal of the American Chemical Society, 2004 , vol. 126, # 22 p. 6895 - 6899
