2-氧代-4-苯基丁酸乙酯合成路线 （共 50 条）
反应条件
in dichloromethane T=35°C; 144 h;
参考文献
Journal of Organic Chemistry, , vol. 53, # 8 p. 1719 - 1722
反应条件
tert.-butylnitrite; 3-chloro-benzenecarboperoxoic acid; isopentyl nitrite 1.) chloroform, 2.) 30 min; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 23, # 17 p. 1875 - 1876
反应条件
1: 93 percent / SOCl2 / 10 h / Ambient temperature 2: 87 percent Chromat. / CrO3-pyridine / CH2Cl2 / 2.5 h / other reagents: K<CrO3Cl>, CrO3/Al2O3 View Scheme
参考文献
Synthetic Communications, , vol. 26, # 11 p. 2229 - 2233
反应条件
1: 1) NaOMe; 2) 15 percent H2SO4 / 1) MeOH, 60-70 deg C, 1.5 h; 2) reflux 15 h 2: ethanol; H2SO4 / 5 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 34, # 3 p. 1128 - 1147
反应条件
water; calcium carbonate; mercury dichloride
参考文献
Tetrahedron Letters, , p. 4657 - 4660
反应条件
in ethanol; sulfuric acid 5 h; Heating; Yield given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 34, # 3 p. 1128 - 1147
反应条件
in diethyl ether Grignard reaction;
参考文献
Tetrahedron Asymmetry, , vol. 10, # 20 p. 3863 - 3867
反应条件
zinc(II) chloride 1.) ether, room temperature, 24 h, 2.) ether, 0 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 32, # 5 p. 1800 - 1807
反应条件
(i) NaH, (ii) /BRN= 1718733/, CuCl2, CuO; Multistep reaction;
参考文献
Tetrahedron Letters, , p. 375 - 378
反应条件
lt;RhTFAlt;Cygt;(AMPP)gt;2; hydrogen in toluene T=20°C; P=38000 Torr; 1.5 h; other glyoxalic acid derivatives, other rhodium catalysts; var. time and pressure; Product distribution;
参考文献
Tetrahedron Asymmetry, , vol. 8, # 7 p. 1083 - 1099
