3-环己烯-1-羧酸甲酯合成路线 （共 53 条）
反应条件
1: 97 percent / H2 / 5percent Rh/Al2O3 / methanol / 24 h / 25 °C / 2585.7 Torr 2: 91.1 percent / diethyl ether / 25 °C 3: 2.0 g / pyridine / benzene / 24 h / 25 °C 4: 62.3 percent / 1,8-dizazabicyclo<5.4.0>undec-7-ene (DBU) / dioxane / 1 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 12 p. 2218 - 2227
反应条件
sulfuric acid Reflux;
参考文献
Srinivasula Reddy; Gangi Reddy; Ram Reddy; Lingappa; Krishna Rao; Damu; Lee, Yong-Ill
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 6 p. 1732 - 1734
反应条件
hydroquinone T=140°C; 8 h; other acrylic acid derivatives and other dienes; calculated ΔH(excit.), lengths of the forming bonds and negative vibrations for the transition states; Thermodynamic data;
参考文献
Branchadell; Oliva; Ortuno; Rafel; Ventura
Tetrahedron, 1992 , vol. 48, # 41 p. 9001 - 9012
反应条件
calcium sulfate; silver(l) oxide 24 h;
参考文献
Tanyeli, Cihangir; Turkut, Engin
Tetrahedron Asymmetry, 2004 , vol. 15, # 13 p. 2057 - 2060
参考文献
Journal of the American Chemical Society, , vol. 79, p. 3098,3101
Journal of the American Chemical Society, , vol. 91, p. 7090,7091
参考文献
Journal of the American Chemical Society, , vol. 79, p. 3098,3101
Journal of the American Chemical Society, , vol. 91, p. 7090,7091
反应条件
1: 91.1 percent / diethyl ether / 25 °C 2: 2.0 g / pyridine / benzene / 24 h / 25 °C 3: 62.3 percent / 1,8-dizazabicyclo<5.4.0>undec-7-ene (DBU) / dioxane / 1 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 12 p. 2218 - 2227
反应条件
1: 2.0 g / pyridine / benzene / 24 h / 25 °C 2: 62.3 percent / 1,8-dizazabicyclo<5.4.0>undec-7-ene (DBU) / dioxane / 1 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 12 p. 2218 - 2227
反应条件
1: 92 percent / pyridine / acetic anhydride / 3 h / Heating 2: 75 percent / aq. NaOH / benzene / 20 h / Ambient temperature 3: 80 percent / H2SO4 / 24 h / Heating 4: 70 percent / NaBH4 / methanol / 4 h / 0 °C 5: 60 percent / pyridine / 1.) 0 deg C, 1 h, 2.) room temperature, 3 h 6: LiI, HMPA / 150 °C View Scheme
参考文献
Synthetic Communications, , vol. 14, # 5 p. 401 - 406
反应条件
1: 70 percent / Na, H2O, EtOH / 24 h / Ambient temperature 2: 92 percent / pyridine / acetic anhydride / 3 h / Heating 3: 75 percent / aq. NaOH / benzene / 20 h / Ambient temperature 4: 80 percent / H2SO4 / 24 h / Heating 5: 70 percent / NaBH4 / methanol / 4 h / 0 °C 6: 60 percent / pyridine / 1.) 0 deg C, 1 h, 2.) room temperature, 3 h 7: LiI, HMPA / 150 °C View Scheme
参考文献
Synthetic Communications, , vol. 14, # 5 p. 401 - 406
