1-甲基环己-3-烯-1-羧酸甲酯合成路线 （共 5 条）
反应条件
1: H2 / Pd-C 2: LiAlH4 / diethyl ether View Scheme
参考文献
Wilcox,C.F.; Chibber,S.S.
Journal of Organic Chemistry, 1962 , vol. 27, p. 2332 - 2338
反应条件
hydroquinone
T=180°C; Diels-Alder reaction;
参考文献
Lawrence, Andrew L.; Lee, Victor; Adlington, Robert M.
Synlett, 2008 , # 14 p. 2087 - 2088
反应条件
sodium hydroxide in water
5 h; Heating;
参考文献
House, Herbert O.; Haack, John L.; McDaniel, William C.; VanDerveer, Don
Journal of Organic Chemistry, 1983 , vol. 48, # 10 p. 1643 - 1654
反应条件
1: LiAlH4 / diethyl ether / Heating
2: NaNO2, H2SO4 / H2O / -10 °C
3: benzene / 10 h / Irradiation
View Scheme
参考文献
Nouguier,R.; Surzur,J.-M.
Bulletin de la Societe Chimique de France, 1973 , p. 2399 - 2403
反应条件
1: 70percent m-chloroperbenzoic acid, NaHCO3 / CHCl3 / 1 h
2: 1.) H2; 2.) Jones reagent / 1.) PtO2 / 1.) AcOH, 50 deg C, 1 atm; 2.) acetone, RT, 30 min
View Scheme
参考文献
Sohda; Meguro; Kawamatsu
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 6 p. 2267 - 2278
