N,N-二甲基-2-吩嗪胺合成路线 （共 3 条）
反应条件
sodium tetrahydroborate in sulfolane
T=120°C; 4 h;
参考文献
Shishkin, G. V.; Sil'nikov, V. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 12 p. 1342 - 1345
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 12 p. 1658 - 1661
反应条件
1: 66 percent / POCl3 / 1.5 h / Heating
2: 0.04 g / NaBH4 / tetrahydrothiophene 1,1-dioxide / 4 h / 120 °C
View Scheme
参考文献
Shishkin, G. V.; Sil'nikov, V. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 12 p. 1342 - 1345
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 12 p. 1658 - 1661
反应条件
1: 61 percent / methanol / 20 °C
2: 66 percent / POCl3 / 1.5 h / Heating
3: 0.04 g / NaBH4 / tetrahydrothiophene 1,1-dioxide / 4 h / 120 °C
View Scheme
参考文献
Shishkin, G. V.; Sil'nikov, V. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 12 p. 1342 - 1345
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 12 p. 1658 - 1661
