3,4-二氯-6-苯基哒嗪合成路线 （共 23 条）
反应条件
phosphorus pentachloride; trichlorophosphate T=120°C; 12 h;
参考文献
Watterson, D. Martin; Van Eldik, Linda; Hu, Wenhui
Patent: US2009/325973 A1, 2009 ;
Location in patent: Page/Page column 39 ;
反应条件
1: sodium acetate / aq. ethanol / 29 h / Heating 2: POCl3; PCl5 / 12 h / 120 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 17, # 2 p. 414 - 418
反应条件
phosphorus pentachloride; trichlorophosphate 8 h; Heating;
参考文献
Sircar
Journal of Heterocyclic Chemistry, 1983 , vol. 20, # 6 p. 1473 - 1476
反应条件
phosphorus pentachloride; trichlorophosphate 8 h; Heating;
参考文献
Sircar
Journal of Heterocyclic Chemistry, 1983 , vol. 20, # 6 p. 1473 - 1476
反应条件
1: 2 g / acetic acid / 6 h / Heating 2: H2 / 10percent Pd-C / tetrahydrofuran View Scheme
参考文献
Sircar
Journal of Heterocyclic Chemistry, 1983 , vol. 20, # 6 p. 1473 - 1476
反应条件
1: 32 percent / acetic acid / 5 h / Heating
2: 97 percent / butan-1-ol / 41 h / 130 °C
View Scheme
参考文献
Hu, Wenhui; Ralay Ranaivo, Hantamalala; Roy, Saktimayee M.; Behanna, Heather A.; Wing, Laura K.; Munoz, Lenka; Guo, Ling; Van Eldik, Linda J.; Watterson, D. Martin
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 2 p. 414 - 418
反应条件
1: 32 percent / acetic acid / 5 h / Heating
2: 97 percent / butan-1-ol / 41 h / 130 °C
3: 91 percent / POCl3 / 3 h / 100 °C
View Scheme
参考文献
Hu, Wenhui; Ralay Ranaivo, Hantamalala; Roy, Saktimayee M.; Behanna, Heather A.; Wing, Laura K.; Munoz, Lenka; Guo, Ling; Van Eldik, Linda J.; Watterson, D. Martin
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 2 p. 414 - 418
反应条件
in ethanol
5 h; steam bath;
参考文献
Sircar
Journal of Heterocyclic Chemistry, 1983 , vol. 20, # 6 p. 1473 - 1476
反应条件
in ethanol
5 h; steam bath;
参考文献
Sircar
Journal of Heterocyclic Chemistry, 1983 , vol. 20, # 6 p. 1473 - 1476
反应条件
in ethanol
5 h; steam bath;
参考文献
Sircar
Journal of Heterocyclic Chemistry, 1983 , vol. 20, # 6 p. 1473 - 1476
