1.1: 97 percent / triethylamine / CH2Cl2 / 3 h / 20 °C
2.1: AlCl3 / 2.5 h / 130 °C
2.2: 97 percent / hydrochloric acid / 0.75 h
3.1: potassium hydroxide / ethanol / 200 h
4.1: 0.777 g / H2O2; NaOH / methanol; H2O / 26 h / 0 °C
View Scheme
参考文献
Bennett, Christopher J.; Caldwell, Stuart T.; McPhail, Donald B.; Morrice, Philip C.; Duthie, Garry G.; Hartley, Richard C.
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 9 p. 2079 - 2098
1.1: AlCl3 / 2.5 h / 130 °C
1.2: 97 percent / hydrochloric acid / 0.75 h
2.1: potassium hydroxide / ethanol / 200 h
3.1: 0.777 g / H2O2; NaOH / methanol; H2O / 26 h / 0 °C
View Scheme
参考文献
Bennett, Christopher J.; Caldwell, Stuart T.; McPhail, Donald B.; Morrice, Philip C.; Duthie, Garry G.; Hartley, Richard C.
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 9 p. 2079 - 2098
1: potassium hydroxide / ethanol / 200 h
2: 0.777 g / H2O2; NaOH / methanol; H2O / 26 h / 0 °C
View Scheme
参考文献
Bennett, Christopher J.; Caldwell, Stuart T.; McPhail, Donald B.; Morrice, Philip C.; Duthie, Garry G.; Hartley, Richard C.
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 9 p. 2079 - 2098
1: potassium hydroxide / ethanol / 200 h
2: 0.777 g / H2O2; NaOH / methanol; H2O / 26 h / 0 °C
View Scheme
参考文献
Bennett, Christopher J.; Caldwell, Stuart T.; McPhail, Donald B.; Morrice, Philip C.; Duthie, Garry G.; Hartley, Richard C.
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 9 p. 2079 - 2098