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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
649569-53-9
合成路线
（共 7 条）
649569-53-9
→
反应条件
40133-14-0
5-(4-氯苯在)噻吩-2-羧酸
反应条件
1.1: H2SO4 / methanol / 1 h / Heating 1.2: chloranil / benzene / 2 h / Heating 2.1: POCl3 / 1,2-dichloro-ethane / 17 h / Heating 3.1: 86 percent / NaOH; Ag2O / H2O / 20 - 50 °C View Scheme
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
649569-53-9
→
反应条件
38401-71-7
5-(4-氯苯基)噻吩-2-甲醛
反应条件
1.1: H2SO4 / methanol / 1 h / Heating 1.2: chloranil / benzene / 2 h / Heating 2.1: POCl3 / 1,2-dichloro-ethane / 17 h / Heating View Scheme
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
108-90-7
氯苯
→
反应条件
649569-53-9
反应条件
1: AlCl3 / CS2 / 2.5 h / 20 °C 2: dimethylformamide / 22 h / 5 °C View Scheme
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
40877-09-6
4,4'-二氯苯丁酮
+
10387-40-3
硫代乙酸钾
→
反应条件
649569-53-9
反应条件
in N,N-dimethyl-formamide T=5°C; 22 h;
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
649569-53-9
→
反应条件
649569-56-2
5-(4-氯苯基)噻吩-2-羧酸甲酯
反应条件
1.1: H2SO4 / methanol / 1 h / Heating 1.2: chloranil / benzene / 2 h / Heating 2.1: POCl3 / 1,2-dichloro-ethane / 17 h / Heating 3.1: 86 percent / NaOH; Ag2O / H2O / 20 - 50 °C 4.1: 86 percent / H2SO4 / toluene / 7 h / Heating View Scheme
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
649569-53-9
→
反应条件
84863-77-4
反应条件
1.1: H2SO4 / methanol / 1 h / Heating 1.2: chloranil / benzene / 2 h / Heating 2.1: POCl3 / 1,2-dichloro-ethane / 17 h / Heating 3.1: 86 percent / NaOH; Ag2O / H2O / 20 - 50 °C 4.1: 86 percent / H2SO4 / toluene / 7 h / Heating 5.1: LiAlH4 / diethyl ether / Heating 6.1: HMPA; thionyl chloride / tetrahydrofuran / 20 °C 7.1: 18-crown-6 / acetonitrile / 20 °C 8.1: KOH / ethanol; H2O / Heating 9.1: 67 percent / H2SO4 / Heating View Scheme
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
649569-53-9
→
反应条件
40133-23-1
2-(4-氯苯基)噻吩
反应条件
1: With sulfuric acid in methanol 1 h; Heating; 2: With chloranil in benzene 2 h; Heating;
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
