beta-甲基-2-硝基-苯乙醇合成路线 （共 12 条）
反应条件
1.1: diethyl ether / 3.5 h / 0 - 20 °C / Inert atmosphere
1.2: Cooling with ice
2.1: toluene-4-sulfonic acid; hydroquinone / benzene / Reflux; Azeotropic water removal
3.1: dimethylsulfide borane complex / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere
3.2: 1 h / 20 - 40 °C
3.3: 20 - 30 °C
View Scheme
参考文献
Serra, Stefano
Tetrahedron Asymmetry, 2011 , vol. 22, # 6 p. 619 - 628
反应条件
1.1: toluene-4-sulfonic acid; hydroquinone / benzene / Reflux; Azeotropic water removal
2.1: dimethylsulfide borane complex / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere
2.2: 1 h / 20 - 40 °C
2.3: 20 - 30 °C
View Scheme
参考文献
Serra, Stefano
Tetrahedron Asymmetry, 2011 , vol. 22, # 6 p. 619 - 628
