2-(3-哌啶基)乙酸乙酯合成路线 （共 7 条）
反应条件
platinum(IV) oxide; hydrogen in acetic acid T=80°C; P=6205.94 Torr; 0.666667 h; Microwave irradiation;
参考文献
Piras, Leonarda; Genesio, Eva; Ghiron, Chiara; Taddei, Maurizio
Synlett, 2008 , # 8 p. 1125 - 1128
反应条件
5 Pd(II)/C(eggshell); hydrogen in ethanol T=20°C; P=7500.75 Torr; 8 h;
参考文献
Zhu, Ying-Guang; Kan, Hong-Zhu; Jiang, Li-Qin; Hu, Wen-Hao
Synthetic Communications, 2012 , vol. 42, # 8 p. 1137 - 1145
反应条件
hydrogen in ethanol; ethyl acetate
参考文献
US5776931 A1, ;
US 5776931 A
反应条件
1: 5 Pd(II)/C(eggshell); hydrogen 2: acetonitrile / 12 h / Reflux 3: 5 Pd(II)/C(eggshell); hydrogen / ethanol / 8 h / 20 °C / 7500.75 Torr View Scheme
参考文献
Synthetic Communications, , vol. 42, # 8 p. 1137 - 1145
反应条件
1: thionyl chloride / 16.25 h / 0 °C / Reflux 2: acetonitrile / 12 h / Reflux 3: 5 Pd(II)/C(eggshell); hydrogen / ethanol / 8 h / 20 °C / 7500.75 Torr View Scheme
参考文献
Synthetic Communications, , vol. 42, # 8 p. 1137 - 1145
反应条件
in dichloromethane T=20°C;
参考文献
Bristol-Myers Squibb Co.
Patent: US6335324 B1, 2002 ;
Location in patent: Page column 257 ;
US 6335324 B1
反应条件
(R)-(-)-α-hydroxybenzeneacetic acid in ethyl acetate 4 h; RefluxResolution of racemate; optical yield given as percent ee;
参考文献
Zhu, Ying-Guang; Kan, Hong-Zhu; Jiang, Li-Qin; Hu, Wen-Hao
Synthetic Communications, 2012 , vol. 42, # 8 p. 1137 - 1145
