1: tetrahydrofuran / 20 h / Ambient temperature 2: 1.) CH3Li / 1.) THF, RT, 15 min, 2.) THF, RT, 3 h View Scheme
参考文献
Ibarra, C. Alvarez; Rodriguez, R. Cuervo; Monreal, M. C. Fernandez; Navarro, F. J. Garcia; Tesorero, J. Martin
Journal of Organic Chemistry, 1989 , vol. 54, # 23 p. 5620 - 5623
1: 2-amino-benzenethiol With 4-methoxytrityl resin chloride; N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 2: benzoic acid With diisopropyl-carbodiimide in N,N-dimethyl-formamide T=20°C; 3 h; 3: With triethylsilane; trifluoroacetic acid in dichloromethane Title compound not separated from byproducts;
Dorofeenko,G.N. et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1971 , vol. 7, p. 319 - 323
Khimiya Geterotsiklicheskikh Soedinenii, 1971 , vol. 7, # 3 p. 345 - 349
