H2O; H2O2 in water 30 min shaking with H2O at 20°C excluding air; dropwise addn. of H2O2; washing (H2O); 5-6 d freeze-drying; sublimation;
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 1.6, page 40 - 51
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Bennett, F. W.; Emeleus, H. J.; Haszeldine, R. N.
Journal of the Chemical Society, 1954 , p. 3598 - 3603
Bennet, F. W.; Emeleus, H. J.; Haszeldine, R. N.
Journal of the Chemical Society, 1953 , p. 1565 - 1571
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Gmelin Handbook: P: MVol.C, 274, page 629 - 631
Harris, G. S.
Journal of the Chemical Society, 1958 , p. 512 - 519
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Gmelin Handbook: F: PerFHalOrg.3, 1.9, page 70 - 123
25°C (3 d); distn. (incomplete sepn. from ((CF3)2P)2NH);
参考文献
Singh,J.; Burg,A.B.
Journal of the American Chemical Society, 1966 , vol. 88, p. 718 - 722
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Gmelin Handbook: F: PerFHalOrg.3, 2.4, page 200 - 203
byproducts: P-O compounds; 25°C (72 h); (CF3)2PCl in no excess;
参考文献
Singh,J.; Burg,A.B.
Journal of the American Chemical Society, 1966 , vol. 88, p. 718 - 722
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Gmelin Handbook: F: PerFHalOrg.3, 2.3, page 196 - 200