1.1: sodium hydroxide / water / 1 h / 20 °C
1.2: 20 - 80 °C
2.1: hydrogenchloride / water / 70 - 80 °C
2.2: 8 h / 80 °C
3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C
3.2: -78 - 20 °C
View Scheme
参考文献
Singh, Anil K.; Khade, Prashant K.
Tetrahedron Letters, 2011 , vol. 52, # 38 p. 4899 - 4902
1.1: hydrogenchloride / water / 70 - 80 °C
1.2: 8 h / 80 °C
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C
2.2: -78 - 20 °C
View Scheme
参考文献
Singh, Anil K.; Khade, Prashant K.
Tetrahedron Letters, 2011 , vol. 52, # 38 p. 4899 - 4902
