5-(羟基甲基)-2-苯并呋喃-1(3H)-酮合成路线 (共 6 条)
反应条件
manganese(IV) oxide in tetrahydrofuran T=20°C; 1 h;
参考文献
Sankyo Company, Limited
Patent: EP1362856 A1, 2003 ;
Location in patent: Page/Page column 113 ;
反应条件
1: With 1,1'-carbonyldiimidazole in tetrahydrofuran
T=20°C; 2 h;
2: With sodium tetrahydroborate in tetrahydrofuran; water
3: With hydrogenchloride in tetrahydrofuran; water
pH=2;
参考文献
PETER MACCALLUM CANCER INSTITUTE; SPICER, Julie Ann; HUTTUNEN, Kristiina Maria; LYONS, Dani Michelle; TRAPANI, Joseph Albert; SMYTH, Mark John; DENNY, William Alexander
Patent: WO2011/75784 A1, 2011 ;
Location in patent: Page/Page column 92-93 ;
反应条件
sulfuric acid in 1,4-dioxane
参考文献
KTB Tumorforschungsgesellschaft mbH
Patent: EP2123305 A1, 2009 ;
反应条件
water; calcium carbonate
参考文献
Perkin; Stone
Journal of the Chemical Society, 1925 , vol. 127, p. 2292
反应条件
water; calcium carbonate
参考文献
Perkin; Stone
Journal of the Chemical Society, 1925 , vol. 127, p. 2292
反应条件
2: calcium carbonate; water
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参考文献
Perkin; Stone
Journal of the Chemical Society, 1925 , vol. 127, p. 2292