1: in tetrahydrofuran
T=-70 - 20°C; 6 h;
2: With ammonium chloride in tetrahydrofuran; water
参考文献
VITAE PHARMACEUTICALS, INC.; CLAREMON, David A.; LEFTHERIS, Katerina; SINGH, Suresh B.; TICE, Colin M.; YE, Yuanjie; ZHUANG, Linghang; ZHAO, Wei
Patent: WO2011/2910 A1, 2011 ;
Location in patent: Page/Page column 79 ;
WO 2011/002910 A1