1,3-二氧戊环-2,2-二乙酸二甲酯合成路线 (共 4 条)
反应条件
hydrogenchloride in tetrahydrofuran; N-methyl-acetamide; acetone
参考文献
Yoshitomi Pharmaceutical Industries, Ltd.
Patent: US5948820 A1, 1999 ;
反应条件
lithium aluminium tetrahydride in tetrahydrofuran Reduction;
参考文献
Tetrahedron Letters, , vol. 41, # 40 p. 7619 - 7622
反应条件
chloro-trimethyl-silane in dichloromethane
Heating;
参考文献
Yadav; Bandyopadhyay; Kunwar
Tetrahedron Letters, 2001 , vol. 42, # 29 p. 4907 - 4911
反应条件
diisobutylaluminium hydride in dichloromethane
T=-78°C; 2 h;
参考文献
Jung, Mankil; Miller, Marvin J.
Tetrahedron Letters, 1985 , vol. 26, # 8 p. 977 - 980