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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
650607-38-8
合成路线
（共 5 条）
850011-22-2
→
反应条件
650607-38-8
反应条件
2-Nitropropane; sodium in ethanol Hass-Bender oxidation; 3 h; Heating;
参考文献
Boa, Andrew N.; Canavan, Shane P.; Hirst, Paul R.; Ramsey, Christopher; Stead, Andrew M.W.; McConkey, Glenn A.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 6 p. 1945 - 1967
850011-21-1
→
反应条件
650607-38-8
反应条件
1: 87 percent / N-bromosuccinimide; benzoyl peroxide / CCl4 / 3 h / Heating 2: 85 percent / 2-nitropropane; sodium / ethanol / 3 h / Heating View Scheme
参考文献
Boa, Andrew N.; Canavan, Shane P.; Hirst, Paul R.; Ramsey, Christopher; Stead, Andrew M.W.; McConkey, Glenn A.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 6 p. 1945 - 1967
174636-75-0
→
反应条件
650607-38-8
反应条件
1: 16 g / CH2Cl2 / 3 h / Heating 2: 87 percent / N-bromosuccinimide; benzoyl peroxide / CCl4 / 3 h / Heating 3: 85 percent / 2-nitropropane; sodium / ethanol / 3 h / Heating View Scheme
参考文献
Boa, Andrew N.; Canavan, Shane P.; Hirst, Paul R.; Ramsey, Christopher; Stead, Andrew M.W.; McConkey, Glenn A.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 6 p. 1945 - 1967
60538-98-9
6-甲基-2-苯基喹啉-4-羧酸
→
反应条件
650607-38-8
反应条件
1: thionyl chloride / 3 h / Heating 2: 16 g / CH2Cl2 / 3 h / Heating 3: 87 percent / N-bromosuccinimide; benzoyl peroxide / CCl4 / 3 h / Heating 4: 85 percent / 2-nitropropane; sodium / ethanol / 3 h / Heating View Scheme
参考文献
Boa, Andrew N.; Canavan, Shane P.; Hirst, Paul R.; Ramsey, Christopher; Stead, Andrew M.W.; McConkey, Glenn A.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 6 p. 1945 - 1967
98-86-2
苯乙酮
→
反应条件
650607-38-8
反应条件
1: 90 percent / potassium hydroxide / H2O; ethanol / 18 h / Heating 2: thionyl chloride / 3 h / Heating 3: 16 g / CH2Cl2 / 3 h / Heating 4: 87 percent / N-bromosuccinimide; benzoyl peroxide / CCl4 / 3 h / Heating 5: 85 percent / 2-nitropropane; sodium / ethanol / 3 h / Heating View Scheme
参考文献
Boa, Andrew N.; Canavan, Shane P.; Hirst, Paul R.; Ramsey, Christopher; Stead, Andrew M.W.; McConkey, Glenn A.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 6 p. 1945 - 1967
