2,5-二甲基-1,3-苯并噻唑-4-胺合成路线 （共 4 条）
反应条件
hydrogen in tetrahydrofuran; ethanol
P=760.051 Torr;
参考文献
STERIX LIMITED
Patent: WO2004/37251 A1, 2004 ;
Location in patent: Page/Page column 103 ;
反应条件
hydrogenchloride; tin(ll) chloride
T=60°C; 2 h;
参考文献
Ryu, Chung-Kyu; Choi, Ko Un; Shim, Ju-Yeon; You, Hea-Jung; Choi, Ik Hwa; Chae, Mi Jin
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 18 p. 4003 - 4008
反应条件
1: 92 percent / HNO3; H2SO4 / 2 h / 20 °C
2: 70 percent / SnCl2; aq. HCl / 2 h / 60 °C
View Scheme
参考文献
Ryu, Chung-Kyu; Choi, Ko Un; Shim, Ju-Yeon; You, Hea-Jung; Choi, Ik Hwa; Chae, Mi Jin
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 18 p. 4003 - 4008
反应条件
potassium dihydrogenphosphate; Fremy’s salt in water
T=20°C; 5 h;
参考文献
Ryu, Chung-Kyu; Choi, Ko Un; Shim, Ju-Yeon; You, Hea-Jung; Choi, Ik Hwa; Chae, Mi Jin
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 18 p. 4003 - 4008
