2,3-二氯-6-硝基苯胺合成路线 （共 14 条）
反应条件
ammonia in methanol T=120°C; 24 h;
参考文献
Saluja; Zou; Drach; Townsend
Journal of Medicinal Chemistry, 1996 , vol. 39, # 4 p. 881 - 891
反应条件
methoxylamine hydrochloride; potassium tert-butylate; copper diacetate in ethylene glycol diethyl ether T=20°C; Substitution; Amination; 2 h;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 11 p. 1437 - 1444
反应条件
1: With sulfuric acid; potassium nitrate T=2 - 5°C; 4 h; 2: With sulfuric acid T=100 - 110°C; 2 h;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 15, # 5 p. 1914 - 1927
反应条件
sulfuric acid; potassium nitrate T=0 - 10°C; Nitration; 4 h; Further byproducts given;
参考文献
Heterocycles, , vol. 53, # 2 p. 423 - 432
反应条件
1.1: 98 percent / 20 °C 2.1: sulfuric acid; potassium nitrate / 4 h / 2 - 5 °C 2.2: 24 percent / sulfuric acid / 2 h / 100 - 110 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 15, # 5 p. 1914 - 1927
参考文献
Gazzetta Chimica Italiana, , vol. 107, p. 175 - 180
反应条件
1: HNO3 2: H2SO4 View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 107, p. 175 - 180
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1107 - 1114
参考文献
Justus Liebigs Annalen der Chemie, , vol. 192, p. 230
参考文献
Beilstein; Kurbatow
Justus Liebigs Annalen der Chemie, 1879 , vol. 196, p. 222
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1879 , vol. 11, p. 332
