1: With 1,3-bis(2,6-diisopropylphenyl)-2-(pentafluorophenyl)imidazolidine; palladium diacetate; sodium t-butanolate in toluene
T=100°C; 18 h; Inert atmosphere;
2: With hydrogenchloride in water; toluene
参考文献
Bedford, Robin B.; Butts, Craig P.; Haddow, Mairi F.; Osborne, Robert; Sankey, Rosalind F.
Chemical Communications, 2009 , # 32 p. 4832 - 4834
1: With 1,3-bis(2,6-diisopropylphenyl)-2-(pentafluorophenyl)imidazolidine; palladium diacetate; sodium t-butanolate in toluene
T=100°C; 18 h; Inert atmosphere;
2: With hydrogenchloride in water; toluene
参考文献
Bedford, Robin B.; Butts, Craig P.; Haddow, Mairi F.; Osborne, Robert; Sankey, Rosalind F.
Chemical Communications, 2009 , # 32 p. 4832 - 4834
1: With 1,3-bis(2,6-diisopropylphenyl)-2-(pentafluorophenyl)imidazolidine; palladium diacetate; sodium t-butanolate in toluene
T=100°C; 18 h; Inert atmosphere;
2: With hydrogenchloride in water; toluene
参考文献
Bedford, Robin B.; Butts, Craig P.; Haddow, Mairi F.; Osborne, Robert; Sankey, Rosalind F.
Chemical Communications, 2009 , # 32 p. 4832 - 4834
Stokes, Benjamin J.; Jovanovic, Brankica; Dong, Huijun; Richert, Kathleen J.; Riell, Ryan D.; Driver, Tom G.
Journal of Organic Chemistry, 2009 , vol. 74, # 8 p. 3225 - 3228
1: 88 percent / H2 / 10 percent palladium on charcoal / ethanol
2: 78 percent / 1M HCl, NaNO2 / ethanol; H2O / 4 h / Ambient temperature
3: 30 percent / 640 °C / 0.03 Torr
View Scheme
参考文献
Kulagowski, Janusz J.; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 2725 - 2732
1: 65 percent / potassium fluoride / 46 h / 190 °C
2: 88 percent / H2 / 10 percent palladium on charcoal / ethanol
3: 78 percent / 1M HCl, NaNO2 / ethanol; H2O / 4 h / Ambient temperature
4: 30 percent / 640 °C / 0.03 Torr
View Scheme
参考文献
Kulagowski, Janusz J.; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 2725 - 2732
