sodium perchlorate T=25°C; Kinetics;

potassium hydroxide in ethanol Heating;

1: 53 percent / KOH / ethanol / Heating 2: 1.) Li, Fe(NO3)3 / 1.) liq.NH3, HMPA, 30 min; 2.) 6 h View Scheme

1: 53 percent / KOH / ethanol / Heating 2: 1.) MeI, Li / 1.) Et2O, 20 deg C, 1 h; 2.) 20 deg C, 12 h View Scheme

1: 53 percent / KOH / ethanol / Heating 2: 1.) MeI, Li / 1.) Et2O, 20 deg C, 1 h; 2.) 20 deg C, 12 h 3: 84 percent / CaCl2, CuCl, Cu, 12N HCl / diethyl ether; petroleum ether / 1 h / 5 °C 4: 1.) Mg / 1.) Et2O; 2.) 12 h, RT; 2 h, reflux View Scheme

hydrogenchloride 96 h;