5,6-环氧-5,6-二氢-[1,10]菲咯啉合成路线 （共 7 条）
反应条件
2,4,6-trimereaptotriazine, trisodium salt, nonahydrate in ethanol
参考文献
Dotsenko, Irina A.; Curtis, Matthew; Samoshina, Nataliya M.; Samoshin, Vyacheslav V.
Tetrahedron, 2011 , vol. 67, # 39 p. 7470 - 7478
反应条件
1: 98 percent / 1a) basic alumina / 1a) CH2Cl2, 10 min, (adsorption), 1b) CH2Cl2, 5.5 h, 2) MeOH, 4 h, (desorption) 2: 70 percent / Attenburrow activated manganese dioxide / CHCl3 / other oxidants: i.e. dichlorodicyanobenzoquinone; nickel peroxide 3: boron trifluoride etherate / CH2Cl2 View Scheme
参考文献
Moody, Christopher J.; Rees, Charles W.; Thomas, Robert
Tetrahedron, 1992 , vol. 48, # 17 p. 3589 - 3602
反应条件
sodium hypochlorite; tetra(n-butyl)ammonium hydrogensulfate in chloroform; water
1 h;
参考文献
Norman, Lewis R.; Carlise, Joseph R.; Concepcion Corbea, Javier Jesus; Rees, William S.; Weck, Marcus
Patent: US2005/112077 A1, 2005 ;
Location in patent: Page/Page column 2; 4 ;
反应条件
industrial bleach (pH 8.2-8.3 with conc. HCl); tetra(n-butyl)ammonium hydrogensulfate in chloroform; water
参考文献
Moody, Christopher J.; Rees, Charles W.; Thomas, Robert
Tetrahedron, 1992 , vol. 48, # 17 p. 3589 - 3602
反应条件
sodium hypochlorite in chloroform; water
参考文献
Antkowiak, Roza; Antkowiak, Wieslaw Z.
Tetrahedron Letters, 1997 , vol. 38, # 10 p. 1857 - 1858
反应条件
hydrogenchloride; sodium hypochlorite; tetra(n-butyl)ammonium hydrogensulfate in chloroform; water
1 h;
参考文献
Antkowiak, Roza; Antkowiak, Wieslaw Z.
Heterocycles, 1998 , vol. 47, # 2 p. 893 - 909
反应条件
sulfuric acid
T=100°C; 1 h;
参考文献
Slough, Greg A.; Krchnak, Viktor; Helquist, Paul; Canham, Stephen M.
Organic Letters, 2004 , vol. 6, # 17 p. 2909 - 2912
