7-甲氧基-3-苯磺酰基-1(3H)-异苯并呋喃酮合成路线 （共 11 条）
反应条件
dihydrogen peroxide in acetic acid 1) RT, 2) reflux; m-chloroperbenzoic acid;
参考文献
Hauser, Frank M.; Rhee, Richard P.
Journal of Organic Chemistry, 1980 , vol. 45, # 15 p. 3061 - 3068
反应条件
1: N-bromosuccinimide, benzoyl peroxide / CCl4 / Heating; Irradiation 2: 9percent HCl / acetic acid / 12 h / Heating 3: 72 percent / p-toluenesulfonic acid / benzene / 3 h / Heating 4: 98 percent / 30percent H2O2 / acetic acid / 1) RT, 2) reflux; m-chloroperbenzoic acid View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 15 p. 3061 - 3068
反应条件
1: 72 percent / p-toluenesulfonic acid / benzene / 3 h / Heating 2: 98 percent / 30percent H2O2 / acetic acid / 1) RT, 2) reflux; m-chloroperbenzoic acid View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 15 p. 3061 - 3068
反应条件
1: 9percent HCl / acetic acid / 12 h / Heating 2: 72 percent / p-toluenesulfonic acid / benzene / 3 h / Heating 3: 98 percent / 30percent H2O2 / acetic acid / 1) RT, 2) reflux; m-chloroperbenzoic acid View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 15 p. 3061 - 3068
反应条件
boron trifluoride diethyl etherate in dichloromethane 12 h; Ambient temperature;
参考文献
Murty, Kadiyala V.S.N.; Pal, Ranjan; Dutta, Kalyani; Mal, Dipakranjan
Synthetic Communications, 1990 , vol. 20, # 11 p. 1705 - 1711
反应条件
1: 92.6 percent / TsOH*H2O / benzene / 2 h / Heating 2: 92.6 percent / mCPBA / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Helvetica Chimica Acta, , vol. 85, # 11 p. 3589 - 3604
反应条件
1: 92.6 percent / TsOH*H2O / benzene / 2 h / Heating 2: 92.6 percent / mCPBA / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Helvetica Chimica Acta, , vol. 85, # 11 p. 3589 - 3604
反应条件
3-chloro-benzenecarboperoxoic acid Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 49, # 2 p. 318 - 325
反应条件
1: 85 percent / LiO-t-Bu / tetrahydrofuran 2: 86 percent / N-bromosuccinimide / H2O; acetone / 1.) 0 deg C, 2.) from 0 deg C to room temp., 1 h 3: 94 percent / BBr3 / CH2Cl2 / 7 h / -50 °C 4: 96 percent / 10percent NaOH / tetrahydrofuran / 0.5 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, p. 383 - 384
反应条件
1: 80 percent / LiO-t-Bu 2: 68 percent / N-bromosuccinimide / H2O; acetone / 1.) 0 deg C, 2.) from 0 deg C to room temp., 1 h 3: 93 percent / BBr3 / CH2Cl2 / 7 h / -50 °C View Scheme
参考文献
Hauser, Frank M.; Prasanna, Subbarao
Journal of Organic Chemistry, 1982 , vol. 47, p. 383 - 384
