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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
651331-49-6
合成路线
（共 11 条）
90734-97-7
4-甲氧基吲哚-3-甲醛
+
98-68-0
4-甲氧基苯磺酰氯
→
反应条件
651331-49-6
反应条件
1: 4-methoxy-1H-indole-3-carbaldehyde With sodium hydroxide in dichloromethane T=20°C; 0.5 h; 2: 4methoxybenzenesulfonyl chloride in dichloromethane T=20°C; 12 h;
参考文献
Meiji Dairies Corporation
Patent: EP1533299 A1, 2005 ;
Location in patent: Page/Page column 11 ;
4837-90-5
4-甲氧基吲哚
→
反应条件
651331-49-6
反应条件
1.1: 85 percent / phosphoryl chloride / 1.5 h / 0 - 40 °C 2.1: NaOH / CH2Cl2 / 0.5 h / 20 °C 2.2: 97 percent / CH2Cl2 / 12 h / 20 °C View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
103260-65-7
4-甲氧基吲哚-2-羧酸
→
反应条件
651331-49-6
反应条件
1.1: 94 percent / Cu; quinoline / 2 h / Heating 2.1: 85 percent / phosphoryl chloride / 1.5 h / 0 - 40 °C 3.1: NaOH / CH2Cl2 / 0.5 h / 20 °C 3.2: 97 percent / CH2Cl2 / 12 h / 20 °C View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
111258-23-2
4-甲氧吲哚-2-羧酸甲脂
→
反应条件
651331-49-6
反应条件
1.1: 99 percent / aq. NaOH / 0.5 h / Heating 2.1: 94 percent / Cu; quinoline / 2 h / Heating 3.1: 85 percent / phosphoryl chloride / 1.5 h / 0 - 40 °C 4.1: NaOH / CH2Cl2 / 0.5 h / 20 °C 4.2: 97 percent / CH2Cl2 / 12 h / 20 °C View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
143702-35-6
→
反应条件
651331-49-6
反应条件
1.1: 88 percent / xylene / 1 h / Heating 2.1: 99 percent / aq. NaOH / 0.5 h / Heating 3.1: 94 percent / Cu; quinoline / 2 h / Heating 4.1: 85 percent / phosphoryl chloride / 1.5 h / 0 - 40 °C 5.1: NaOH / CH2Cl2 / 0.5 h / 20 °C 5.2: 97 percent / CH2Cl2 / 12 h / 20 °C View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
135-02-4
2-甲氧基苯甲醛
→
反应条件
651331-49-6
反应条件
1.1: 68 percent / methanol / 1.5 h / -10 °C 2.1: 88 percent / xylene / 1 h / Heating 3.1: 99 percent / aq. NaOH / 0.5 h / Heating 4.1: 94 percent / Cu; quinoline / 2 h / Heating 5.1: 85 percent / phosphoryl chloride / 1.5 h / 0 - 40 °C 6.1: NaOH / CH2Cl2 / 0.5 h / 20 °C 6.2: 97 percent / CH2Cl2 / 12 h / 20 °C View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
651331-49-6
→
反应条件
651331-65-6
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 0.25 h / 0 °C 1.2: potassium tert-butoxide / tetrahydrofuran; hexane / 0.25 h / 0 °C 1.3: 74 percent / tetrahydrofuran; hexane / 2.5 h / -78 - 0 °C 2.1: 93 percent / H2 / Pd/C / ethanol / 4 h / 20 °C / 760 Torr View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
651331-49-6
→
反应条件
651331-68-9
反应条件
1.1: n-BuLi; potassium tert-butoxide / tetrahydrofuran; hexane / 0 °C 1.2: 71 percent / tetrahydrofuran; hexane / -78 - 0 °C 2.1: 94 percent / H2 / Pd/C / ethanol / 20 °C / 760 Torr View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
651331-49-6
→
反应条件
651331-69-0
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 0 °C 1.2: potassium tert-butoxide / tetrahydrofuran; hexane / 0 °C 1.3: 45 percent / tetrahydrofuran; hexane / -78 - 0 °C 2.1: 57 percent / H2 / Pd/C / ethanol / 20 °C / 760 Torr View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
651331-49-6
→
反应条件
651331-70-3
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 0 °C 1.2: potassium tert-butoxide / tetrahydrofuran; hexane / 0 °C 1.3: 69 percent / tetrahydrofuran; hexane / -78 - 0 °C 2.1: 47 percent / H2 / Pd/C / ethanol / 20 °C / 760 Torr View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
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