2-甲基-6,7-二甲氧基-1,2,3,4-四氢异喹啉-1-酮合成路线 （共 61 条）
反应条件
rat liver enzymes; AgCl
1) methanol, 2) 37 deg C, 2 h, pH 7.5; Yield given. Multistep reaction;
参考文献
Walterova; Preininger; Dolejs; et al.
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 3 p. 956 - 965
反应条件
EDTA-activated Gatterman copper; sulfuric acid; sodium nitrite
1.) AcOH, RT, 45 min, 2.) acetone, reflux, 0.5 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Wert, Kathleen L.; Chackalamannil, Samuel; Miller, Eric; Dalton, David R.; Zacharias, David E.; Glusker, Jenny P.
Journal of Organic Chemistry, 1982 , vol. 47, # 26 p. 5141 - 5150
反应条件
EDTA-activated Gatterman copper; sulfuric acid; sodium nitrite
1.) AcOH, RT, 45 min, 2.) acetone, reflux, 0.5 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Wert, Kathleen L.; Chackalamannil, Samuel; Miller, Eric; Dalton, David R.; Zacharias, David E.; Glusker, Jenny P.
Journal of Organic Chemistry, 1982 , vol. 47, # 26 p. 5141 - 5150
反应条件
sodium tetrahydroborate; Fremy’s salt; anhydrous carbonate
1.)ethanol, water, 24 h; Multistep reaction;
参考文献
Castedo, Luis; Puga, Alberto; Saa, Jose M.; Suau, Rafael
Tetrahedron Letters, 1981 , vol. 22, # 23 p. 2233 - 2236
反应条件
alkaline potassium permanganate
参考文献
Pyman
Journal of the Chemical Society, 1910 , vol. 97, p. 275
反应条件
in methanol; diethyl ether
48 h;
参考文献
Bick, I. Ralph C.; Sevenet, Thierry; Sinchai, Wannee; Skelton, Brian W.; White, Allan H.
Australian Journal of Chemistry, 1981 , vol. 34, # 1 p. 195 - 207
反应条件
rat liver enzymes; AgCl
1) methanol, 2) 37 deg C, 2 h, pH 7.5; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Walterova; Preininger; Dolejs; et al.
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 3 p. 956 - 965
反应条件
potassium tert-butylate; dimethyl sulfoxide
24 h; Ambient temperatureOther reagent: NaH/DMSO; Yield given;
参考文献
Barker, John M.; Huddleston, Patrick R.; Clephane, Janette; Wood, Michael L.; Holmes, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 275 - 282
反应条件
trichlorophosphate
1) reflux, 1 h; 2) methylene chloride, 0 deg C, overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Irie, Hiroshi; Shiina, Ayako; Fushimi, Tamaki; Katakawa, Jun'ichi; Fujii, Nobutaka; Yajima, Haruaki
Chemistry Letters, 1980 , p. 875 - 878
反应条件
rat liver enzymes; AgCl
1) methanol, 2) 37 deg C, 2 h, pH 7.5; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Walterova; Preininger; Dolejs; et al.
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 3 p. 956 - 965
