2-氟-3,5-二甲氧基-苯甲酸合成路线 （共 3 条）
反应条件
1: With sodium hydroxide in ethanol
24 h; Heating / reflux;
2: With hydrogenchloride in water
参考文献
Chivikas Connolly, Cleo J.; Deur, Christopher James; Hamby, James Marino; Hoyer, Denton Wade; Limberakis, Chris; Reed, Jessica Elizabeth; Schroeder, Mel Conrad; Taylor, Clarke
Patent: US2004/19210 A1, 2004 ;
Location in patent: Page 13 ;
US 20040019210 A1
反应条件
diphenyl phosphoryl azide; triethylamine in toluene
T=60 - 70°C; 1 h;
参考文献
WARNER-LAMBERT COMPANY LLC
Patent: WO2006/38112 A1, 2006 ;
Location in patent: Page/Page column 29 ;
WO 2006/038112 A1
反应条件
triethylamine in toluene
T=60 - 70°C; 1 h; Heating / reflux;
参考文献
Chivikas Connolly, Cleo J.; Deur, Christopher James; Hamby, James Marino; Hoyer, Denton Wade; Limberakis, Chris; Reed, Jessica Elizabeth; Schroeder, Mel Conrad; Taylor, Clarke
Patent: US2004/19210 A1, 2004 ;
Location in patent: Page 13 ;
US 20040019210 A1
