1: H2, 10percent ethanolic NH3 / Rh/C / 80 °C / 43440.4 Torr 2: 67 percent / 3-methyl-butan-1-ol / 12 h / Heating View Scheme

1: Et3N / tetrahydrofuran / 1 h / Ambient temperature 2: H2, 10percent ethanolic NH3 / Rh/C / 80 °C / 43440.4 Torr 3: 67 percent / 3-methyl-butan-1-ol / 12 h / Heating View Scheme

in 3-methyl-1-butanol 12 h; Heating;