3,4,5,6-四氟邻苯二甲酸合成路线 （共 39 条）
反应条件
hydrogenchloride; potassium fluoride in tetrahydrofuran; sulfolane
参考文献
Warner-Lambert Company
Patent: US4782180 A1, 1988 ;
参考文献
SDS Biotech K.K.
Patent: US4769493 A1, 1988 ;
参考文献
Journal of the Chemical Society, , p. 3372 - 3379
反应条件
hydrogenchloride; sulfuric acid in water; acetic acid
反应条件
SbF5; silica gel T=75°C; 8 h; Overall yield = 0.242g;
参考文献
Journal of Fluorine Chemistry, , vol. 145, p. 41 - 50
反应条件
CaH2; KF; sulfuric acid in tetrahydrofuran; sulfolane; water
反应条件
SbF5; trifluoroacetic acid T=95°C; 28 h;
参考文献
Zonov, Yaroslav V.; Karpov, Victor M.; Platonov, Vyacheslav E.
Journal of Fluorine Chemistry, 2007 , vol. 128, # 9 p. 1058 - 1064
反应条件
1: With bromine T=130°C; 17.5 h; 2: With hydrogenchloride 120 h; Further stages.;
参考文献
Zonov; Karpov; Platonov; Gatilov
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 2 p. 202 - 217
反应条件
1: With SbF5; silica gel T=70°C; 5 h; 2: With hydrogenchloride Further stages.;
参考文献
Russian Journal of Organic Chemistry, , vol. 44, # 2 p. 202 - 217
反应条件
sulfuric acid 3 h; Heating;
参考文献
Dmowski, Wojciech; Wielgat, Jerzy
Journal of Fluorine Chemistry, 1988 , vol. 41, p. 241 - 246
