3,4,5,6-四氟邻苯二甲酸合成路线 （共 39 条）
反应条件
dihydrogen peroxide in acetonitrile T=100°C; 30 h; var. conc.; Product distributionMechanism;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 22, # 12 p. 2307 - 2313
Zhurnal Organicheskoi Khimii, , vol. 22, # 12 p. 2571 - 2578
反应条件
2: 83 percent Spectr. / Zn; NH3; H2O / 29 h / 20 °C View Scheme
参考文献
Konovalov, Valery V.; Laev, Sergey S.; Beregovaya, Irina V.; Shchegoleva, Lyudmila N.; Shteingarts, Vitalij D.; Tsvetkov, Yuri D.; Bilkis, Itzhak
Journal of Physical Chemistry A, 2000 , vol. 104, # 2 p. 352 - 361
反应条件
thionyl chloride T=90°C; 14 h;
参考文献
Tannaci, John F.; Noji, Masahiro; McBee, Jennifer; Tilley, T. Don
Journal of Organic Chemistry, 2007 , vol. 72, # 15 p. 5567 - 5573
反应条件
in methanol; sulfuric acid
参考文献
Daiichi Pharmaceutical Co., Ltd.
Patent: US5849757 A1, 1998 ;
参考文献
Medina, Carlos Perez; Lopez, Concepcion; Claramunt, Rosa M.; Elguero, Jose
European Journal of Organic Chemistry, 2010 , # 5 p. 890 - 899
反应条件
1: ammonia / 100 h / 110 °C / Autoclave 2: sulfuric acid; ammonium chloride; triethylamine / water / 170 h / 130 °C / Sealed tube View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 135, p. 129 - 136
反应条件
1: SO3/H2SO4 2: NH3 / ethanol View Scheme
参考文献
Coe,P.L. et al.
Tetrahedron, 1967 , vol. 23, p. 505 - 508
反应条件
1: SO3/H2SO4 2: LiAlH4 / diethyl ether 3: aq. HBr, H2SO4 View Scheme
参考文献
Kotha, Sambasivarao; Misra, Shilpi; Srinivas, Venu
European Journal of Organic Chemistry, 2012 , # 21 p. 4052 - 4062
反应条件
sulfur(IV) fluoride; hydrogen fluoride T=300°C; 20 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Dmowski, Wojciech
Journal of Fluorine Chemistry, 1993 , vol. 60, # 2.3 p. 251 - 255
