1,2,3,4,5-五氟-6-(三氟乙烯基)苯合成路线 （共 16 条）
反应条件
bis(dibenzylideneacetone)-palladium(0); tri-iso-propyl phosphine in tetrahydrofuran; THF-d8 (tetrahydrofuran-d8)
T=100°C; P=2660.18 Torr; 5 h;
参考文献
Ohashi, Masato; Saijo, Hiroki; Shibata, Mitsutoshi; Ogoshi, Sensuke
European Journal of Organic Chemistry, 2013 , # 3 p. 443 - 447
反应条件
copper in isobutyramide
T=120°C; 5 h;
参考文献
Wlassics, Ivan; Tortelli, Vito
Collection of Czechoslovak Chemical Communications, 2008 , vol. 73, # 12 p. 1719 - 1728
反应条件
T=575 - 580°C; P=0.1 Torr; 0.000138889 h; reaction in a silica tube; Further byproducts given;
参考文献
Barlow, Michael G.; Crawley, Michael W.; Haszeldine, Robert N.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 122 - 125
反应条件
CuC6F5 dioxanate in tetrahydrofuran
byproducts: C6F5I, (C6F5)2; reaction under reflux, 18 hours;;
参考文献
Gmelin Handbook: F: PerFHalOrg.4, 2.2.4, page 68 - 115
反应条件
1,1,2,2-tetrafluoroethylene
T=620°C; Further byproducts given;
参考文献
Dvornikova, K. V.; Platonov, V. E.; Yakobson, G. G.
Russian Chemical Bulletin, 1993 , vol. 42, # 10 p. 1690 - 1693
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 10 p. 1767 - 1770
参考文献
Wlassics, Ivan; Tortelli, Vito
Collection of Czechoslovak Chemical Communications, 2008 , vol. 73, # 12 p. 1719 - 1728
反应条件
1,1,2,2-tetrafluoroethylene
T=530°C; Further byproducts given;
参考文献
Dvornikova, K. V.; Platonov, V. E.; Yakobson, G. G.
Russian Chemical Bulletin, 1993 , vol. 42, # 10 p. 1690 - 1693
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 10 p. 1767 - 1770
反应条件
1: 11 percent / 530 °C
2: PCl5 / 8 h / 230 - 250 °C
3: 5 percent / CF2=CF2 / 620 °C
View Scheme
参考文献
Dvornikova, K. V.; Platonov, V. E.; Yakobson, G. G.
Russian Chemical Bulletin, 1993 , vol. 42, # 10 p. 1690 - 1693
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 10 p. 1767 - 1770
参考文献
Tamborski,C. et al.
Journal of Organometallic Chemistry, 1968 , vol. 15, p. 494 - 496
参考文献
Dvornikova,K.V.; Platonov,V.E.
Journal of Fluorine Chemistry, 1985 , vol. 28, p. 99
