2,3,4,5,6-五氟苯甲酰胺合成路线 (共 28 条)
反应条件
1: pyridine / benzene 2: Na2CO3 / not given View Scheme
参考文献
F: PerFHalOrg.9, 7, page 50 - 101
反应条件
[Ru(η6-C6Me6)Cl2(tris(dimethylamino)phosphine)]; water T=100°C; 0.0833333 h; Inert atmosphereSealed tube;
参考文献
Garcia-Alvarez, Rocio; Zablocka, Maria; Crochet, Pascale; Duhayon, Carine; Majoral, Jean-Pierre; Cadierno, Victorio
Green Chemistry, 2013 , vol. 15, # 9 p. 2447 - 2456
反应条件
[Ru(η6-C6Me6)Cl2(tris(dimethylamino)phosphine)]; hydroxylamine hydrochloride; sodium hydrogencarbonate in water T=100°C; 7 h; Inert atmosphereSealed tubeGreen chemistry; Reagent/catalyst;
参考文献
Garcia-Alvarez, Rocio; Diaz-Alvarez, Alba E.; Crochet, Pascale; Cadierno, Victorio
RSC Advances, 2013 , vol. 3, # 17 p. 5889 - 5894
反应条件
[RuCl2(η2-C6H6){P(NMe2)3}]; water T=100°C; 1 h; Inert atmosphereSealed tube;
参考文献
Garcia-Alvarez, Rocio; Diaz-Alvarez, Alba E.; Borge, Javier; Crochet, Pascale; Cadierno, Victorio
Organometallics, 2012 , vol. 31, # 17 p. 6482 - 6490
参考文献
Dewis, Mark L.; Merrit, Debra; Miller, Kevin; Chen, Zhen; Reiber, Laurens
Patent: US2009/47379 A1, 2009 ;
参考文献
Utkina; Michurin; Shishulina
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 6 p. 889 - 894
反应条件
pyridine in dichloromethane T=0°C; 1 h;
参考文献
Zibarev, A. V.; Dolenko, G. N.; Krupoder, S. A.; Mazalov, L. N.; Poleshchuk, O. Kh.; et al.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 347 - 354
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 2 p. 390 - 398
反应条件
1: With ammonia in methanol 1.5 h; Irradiation; 2: in methanol 24 h;
参考文献
Tetrahedron, , vol. 57, # 27 p. 5865 - 5871
反应条件
2: Na2CO3 / not given View Scheme
参考文献
F: PerFHalOrg.9, 7, page 50 - 101