2,3,5,6-四氟对苯二甲酸合成路线 (共 30 条)
反应条件
water; SbF5; silica gel 1.) 130 deg C, 3.5 h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 27, p. 1932 - 1938
Zhurnal Organicheskoi Khimii, , vol. 27, p. 2183 - 2191
反应条件
potassium permanganate; sodium carbonate
参考文献
Journal of the Chemical Society, , p. 808 - 817
反应条件
1: 7.09 g / SOCl2, DMF / 3 h / 80 - 110 °C 2: 3.14 g / KF / 16 h / 200 °C 3: 1.) SbF5, 2.) H2O / 1.) 130 deg C, 10 h View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 27, p. 1932 - 1938
Zhurnal Organicheskoi Khimii, , vol. 27, p. 2183 - 2191
反应条件
1: 3.14 g / KF / 16 h / 200 °C 2: 1.) SbF5, 2.) H2O / 1.) 130 deg C, 10 h View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 27, p. 1932 - 1938
Zhurnal Organicheskoi Khimii, , vol. 27, p. 2183 - 2191
反应条件
1: Br2 / Irradiation 2: aq. KMnO4, Na2CO3 View Scheme
参考文献
Journal of the Chemical Society, , p. 808 - 817
反应条件
water; SbF5 1.) 130 deg C, 10 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 27, p. 1932 - 1938
Zhurnal Organicheskoi Khimii, , vol. 27, p. 2183 - 2191
反应条件
1: (hydrolysis) 2: (hydrolysis) View Scheme
参考文献
Journal of the Chemical Society, , p. 3372 - 3379
参考文献
US6342602 B1, ;
Page column 26 ;
参考文献
Journal of the Chemical Society, , p. 3372 - 3379
参考文献
F: PerFHalOrg.9, 7, page 50 - 101