3,6-二氟邻苯二甲酸酐合成路线 （共 15 条）
反应条件
AlCl3, aluminium chloride; sodium chloride T=220°C; 3 h;
参考文献
SCHOOL OF PHARMACY, UNIVERSITY OF LONDON
Patent: WO2005/61453 A1, 2005 ;
Location in patent: Page/Page column 19 ;
反应条件
hydrogenchloride; hydroquinone; sodium chloride; AlCl3
参考文献
BTG International Limited
Patent: US6320063 B1, 2001 ;
反应条件
aluminium trichloride; sodium chloride Heating;
参考文献
Krapcho, A. Paul; Getahun, Zelleka; Avery, Kenneth J.
Synthetic Communications, 1990 , vol. 20, # 14 p. 2139 - 2146
反应条件
1: 89 percent / AlCl3, NaCl / 1.5 h / 220 °C
2: 78 percent / pyridine / 48 h / Ambient temperature
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参考文献
Krapcho, A. Paul; Getahun, Zelleka; Avery, Kenneth J.
Synthetic Communications, 1990 , vol. 20, # 14 p. 2139 - 2146
反应条件
1: 72.8 percent / AlCl3 / 12 h / Heating
2: 91 percent / H2SO4 / 1 h / 60 °C
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参考文献
Cardia, Maria Cristina; Begala, Michela; DeLogu, Alessandro; Maccioni, Elias
Farmaco, 2001 , vol. 56, # 8 p. 549 - 554
