邻氨基-N,N-二甲基苯甲酰胺合成路线 （共 10 条）
反应条件
copper acetylacetonate; sodium tetrahydroborate in ethanol 2 h; Ambient temperature;
参考文献
Murphy, John A.; Roome, Stephen J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 11 p. 1349 - 1358
反应条件
in diethyl ether T=0 - 10°C; 0.5 h;
参考文献
Mahiwal, Kuldeep; Kumar, Pradeep; Narasimhan, Balasubramanian
Medicinal Chemistry Research, 2012 , vol. 21, # 3 p. 293 - 307
反应条件
1: (COCl)2 / CH2Cl2 / 2 h / Ambient temperature 2: aq. NaOH / dioxane / 1 h / Ambient temperature 3: H2 / 5percent Pd/C / ethanol / 26 h View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 40, # 17 p. 2674 - 2687
反应条件
1: aq. NaOH / dioxane / 1 h / Ambient temperature 2: H2 / 5percent Pd/C / ethanol / 26 h View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 40, # 17 p. 2674 - 2687
反应条件
in tetrahydrofuran; pentane Ambient temperature;
参考文献
Riviere-Baudet; Morere; Dias
Tetrahedron Letters, 1992 , vol. 33, # 43 p. 6453 - 6456
反应条件
1: thionyl chloride / 4.5 h / 80 °C 2: diethyl ether / 0.5 h / 0 - 10 °C View Scheme
参考文献
Medicinal Chemistry Research, , vol. 21, # 3 p. 293 - 307
反应条件
humic acid in water radical reaction; Irradiation;
参考文献
Pesticide Science, , vol. 46, # 2 p. 151 - 155
反应条件
in water radical reaction; Irradiation;
参考文献
Pesticide Science, , vol. 46, # 2 p. 151 - 155
反应条件
1: 95 percent / Ambient temperature; for 2-7 days 2: 45 percent / LDA / tetrahydrofuran / 0 deg C to room temp., 8-12 h View Scheme
参考文献
Chong, R.J.; Siddiqui, M.A.; Snieckus, V.
Tetrahedron Letters, 1986 , vol. 27, # 44 p. 5323 - 5326
反应条件
1: 68 percent / tetrafluoroboric acid, sodium nitrite / H2O / 0.5 h / -10 °C
2: 39 percent / tetrathiafulvalene / acetone / 2 °C
View Scheme
参考文献
Murphy, John A.; Roome, Stephen J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 11 p. 1349 - 1358
